HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 18996272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 18996271 | HCID 18996271 | — |
| Product | HCID 18996272 | HCID 18996272 | 80% |
Reaction Steps
Using an analogous procedure to that described in Example 68, 4'-[4-(2,2-diethyl-4-methyl-1,3-dioxolan-4-yl)thien-2-ylthio]acetophenone was reacted with hydroxylamine hydrochloride to give (E)-4'-[4-(2,2-diethyl-4-methyl-1,3-dioxolan-4-yl)thien-2-ylthio]acetophenone oxime in 80% yield as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482966 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-ff53eb5c8b394ac0b6e0cf6c9c306ef2 |
| Source note | uspto-grants-1996_01 |