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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 37513Generated: October 29, 2026

3,4-Dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine → HCID 15289707, compound

https://huagongshe.com/reaction/37513

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-Dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridineHCID 19935579—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 15289707HCID 15289707—

Reaction Steps

In 5 ml of ethyl acetate was dissolved 350 mg of 3,4-dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine, and 300 mg of 10% Pd-C (50% wet) was added to the solution. Catalytic reduction reaction was conducted for 4.5 hours. After the reaction mixture was dried over magnesium sulfate, the solvent was distilled off to afford an oily product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05420275
Source datasetuspto-grants-1995_05
ORD IDord-c41010b4ebab483b8d14b7720d002562
Source noteuspto-grants-1995_05