HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine → HCID 15289707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine | HCID 19935579 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15289707 | HCID 15289707 | — |
Reaction Steps
In 5 ml of ethyl acetate was dissolved 350 mg of 3,4-dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine, and 300 mg of 10% Pd-C (50% wet) was added to the solution. Catalytic reduction reaction was conducted for 4.5 hours. After the reaction mixture was dried over magnesium sulfate, the solvent was distilled off to afford an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420275 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-c41010b4ebab483b8d14b7720d002562 |
| Source note | uspto-grants-1995_05 |