HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18994418, compound → HCID 18994392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18994418 | HCID 18994418 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Product | HCID 18994392 | HCID 18994392 | 75% |
Reaction Steps
Using the procedure described in Example 18, 4-[5-(4-(2,3,4,5,6-pentafluoro-alpha-hydroxybenzyl)phenylthio)thien-2-yl]-4-methoxytetrahydropyran was reacted with pyridinium chlorochromate to give 4-[5-(4-(2,3,4,5,6-pentafluorobenzoyl)phenylthio)thien-2-yl]-4-methoxytetrahydropyran in 75% yield, m.p. 93°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484805 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-ba5d7dce0719490497dd004babf9f680 |
| Source note | uspto-grants-1996_01 |