HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18994412, compound → HCID 18994400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18994412 | HCID 18994412 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Product | HCID 18994400 | HCID 18994400 | 75% |
Reaction Steps
Using the procedure described in Example 18, 4-[5-(4-(alphahydroxy-4-trifluoromethylbenzyl)phenylthio)thien-2-yl]-4-methoxytetrahydropyran was reacted with pyridinium chlorochromate to give 4-[5-(4-(4-trifluoromethylbenzoyl)phenylthio)thien-2-yl]-4-methoxytetrahydropyran in 75% yield, m.p. 86°-87° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484805 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-5a64ea34986f45ecbe17b2431fe083d5 |
| Source note | uspto-grants-1996_01 |