HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 3-(3-nitrophenyl)- → 151539-32-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 3-(3-nitrophenyl)- | HCID 68390 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 151539-32-1 | HCID 5368233 | 57% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 4.0 g (17.7 mmol) of 5,6-diamino-1,3-dipropyluracil and 3.8 g (19.5 mmol) of 3-nitrocinnamic acid. Then, the resultant crude crystals were recrystallized from toluene to give 3.86 g (yield 57%) of Compound 34 as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-6d9e2a21d0b341a7b707913264eedcc6 |
| Source note | uspto-grants-1996_01 |