HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)cinnamic acid → 155271-92-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)cinnamic acid | HCID 73778 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 155271-92-4 | HCID 6448938 | 52.1% |
Reaction Steps
Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 3.30 g (17.3 mmol) of 4-(N,N-dimethylamino)cinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 2.78 g (yield 52%) of Compound 162 as yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-9c032572f6674aab9435b7ae73bf2a99 |
| Source note | uspto-grants-1996_01 |