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HRID375418

反应详情

EQUATION

反应方程式

HRID 375418 的结构方程式

REACTANTS

反应物

3
结构：NCCO
HCID700

Ethanolamine

C2H7NO

结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：ClC(c1ccccc1)(c1ccccc1)c1ccccc1
HCID6456

Trityl chloride

C19H15Cl

PRODUCTS

生成物

1
结构：OCCNC(c1ccccc1)(c1ccccc1)c1ccccc1
HCID3125608

2-(tritylamino)ethanol

C21H21NO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of ethanolamine, trityl chloride and pyridine was refluxed for 15 h. Water was added slowly to the cooled reaction and the precipitate collected by filtration. The crude product recrystallized from a 1:1 mixture of ethanol and water.

WORKUP

后处理

  1. temperaturewas refluxed for 15 h
  2. filtrationthe precipitate collected by filtration
  3. customThe crude product recrystallized from a 1:1 mixture of ethanol and water