HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67742921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18993316 | HCID 18993316 | — |
| Product | HCID 67742921 | HCID 67742921 | 98% |
Reaction Steps
A solution of 3-(2,2-diphenyl-2-hydroxyethyl)-1-(3,4-methylenedioxyphenethyl)piperidine hydrate (162 mg) (Example 3) in 2M hydrochloric acid (4.5 ml) was heated at 100° C. for 30 minutes and evaporated to give the title compound as a colourless foam (165 mg, 98%), which was characterised as a hydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05486527 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-626b2b31ea914ddbb88278f8e27a28e4 |
| Source note | uspto-grants-1996_01 |