Cyanuric chloride → 4,6-dichloro-2-ethoxycarbonylmethylamino-S-triazine

Participants

Reaction Steps

36.9 g of cyanuric chloride, 27.9 g of ethyl glycinate hydrochloride and 33.6 g of sodium bicarbonate were heated under reflux in 200 ml of dioxane for 30 minutes. At the end of this time, the dioxane was removed by distillation under reduced pressure, and a mixture of ethyl acetate and water was added to the resulting residue, after which the mixture was shaken.

Provenance & Evidence