HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 18991206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | (2,6-Di-tert-butyl-4-bromophenoxy)trimethylsilane | HCID 10882840 | — |
| Product | HCID 18991206 | HCID 18991206 | 45% |
Reaction Steps
By proceeding as indicated in the procedure of Preparation VII above, starting with 10 mmol of 3,5-di-t-butyl-4-trimethylsilyloxy-bromobenzene and 15 mmol of HCHO (in the protected form of H2C(OCH3)2), one obtains (yield: 45%) 3,5-di-t-butyl-4-trimethylsilyloxy-benzaldehyde, followed by the expected product, 3,5-di-t-butyl-4-hydroxybenzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05487893 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-af45e39ef51a45c29ee659f8040b5eec |
| Source note | uspto-grants-1996_01 |