4-Methoxybenzaldehyde → HCID 6994164, compound

HRID 375825Notes

Reaction equation

HRID 375825 reaction equation
C(=O)[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.CCO[C:14]([CH3:16])=[O:15].[CH3:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[O:15]1[CH2:14][C@H:16]1[CH2:9][O:8][C:5]1[CH:4]=[CH:3][CH:2]=[CH:7][C:6]=1[C:19]1[CH:18]=[CH:17][CH:22]=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 312444-MethoxybenzaldehydeHCID 21226206Ethyl acetate hexane

Product 1

HCID 6994164HCID 6994164, compound

Procedure

13C NMR (CDCl3): δ155, 148, 132, 129, 128, 127, 126, 121,113, 69, 50, 44. TLC: Rf =0.5 in 25% EtOAc/hexane, p-anisaldehyde stain, UV.

Sources & evidence

ORD record
ord-d2682258e1294827a5c9d1a12cb5f661
Source dataset
uspto-grants-1996_01
Patent number
US05488064

Reaction notes

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