HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18914706, compound → HCID 15296673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18914706 | HCID 18914706 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15296673 | HCID 15296673 | — |
Reaction Steps
The title compound of Step 16 (167 mg, 0.4 mmol) is debenzylated in ethanol with 5psi H2 at room temperature for 1.5 hours using 4% Pd/C catalyst. After filtering, the solvent is stripped off to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05488066 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-6073358a46844f67b2197e096a8fc42f |
| Source note | uspto-grants-1996_01 |