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HRID3760

反应详情

EQUATION

反应方程式

HRID 3760 的结构方程式

REACTANTS

反应物

3
结构：Clc1nc(Cl)nc(Cl)n1
HCID7954

2,4,6-Trichloro-s-triazine

C3Cl3N3

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：CCC(C)NCCN1CC(C)(C)NC(C)(C)C1=O
HCID54471771

1-{2-[(Butan-2-yl)amino]ethyl}-3,3,5,5-tetramethylpiperazin-2-one

C14H29N3O

PRODUCTS

生成物

1
结构：CCC(C)N(CCN1CC(C)(C)NC(C)(C)C1=O)c1nc(Cl)nc(Cl)n1
HCID53729334

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

2 次

结构：O
溶剂HCID962

Water

H2O

3 次

PROCEDURE

实验过程

In a 1 liter three-necked flask were placed 300 ml of water which was cooled to 1° C. 46.1 g (0.25 mole) of cyanuric chloride was dissolved in 240 ml acetone and added to the water in the flask. A white slurry formed which was stirred while adding to it dropwise, 63.9 g (0.25 mole) of 1-[2-(2-butylamino)ethyl]-3,3,5,5-tetramethyl-2-piperazinone in 60 ml acetone and 13.3 g of sodium carbonate in 60 ml water. The addition took about 30 min.

WORKUP

后处理

  1. customIn a 1 liter three-necked flask were placed
  2. customA white slurry formed which
  3. additionwhile adding to it dropwise
  4. additionThe addition