HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178419958, compound → HCID 178519547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178419958 | HCID 178419958 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 178519547 | HCID 178519547 | — |
Reaction Steps
The deprotection of the acetal function of 2-[1,3]dioxolan-2-yl-6-(1H-pyrazol-3-yl)pyridine is carried out on 0.65 g of product (2.99 mmol) according to a protocol similar to that used in stage 5 of Example 7. The title compound is isolated by chromatography on a silica column (eluent: chloroform/methanol; 98:2). 0.31 g of a white foam is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06020345 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-6523bea7e44041348a28111cf7835db9 |
| Source note | uspto-grants-2000_02 |