HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86753981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Lysine Monohydrate | HCID 16211825 | — |
| Reactant | HCID 73605422 | HCID 73605422 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86753981 | HCID 86753981 | — |
Reaction Steps
30 g (0.097 mol) of N-(4-trifluoromethylphenyl)-2-cyano-3-hydroxy-hept-2-en-6-ynecarboxamide are dissolved in 1 l of water and 25 ml of ethanol together with 17.3 g (0.097 mol) of L-lysine hydrate, filtered and lyophilized. Adhering residual amounts of ethanol are removed by repeated freeze drying.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06020372 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-4d88d0854589486593b715016d6356a5 |
| Source note | uspto-grants-2000_02 |