HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 70185499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Lysine Monohydrate | HCID 16211825 | — |
| Reactant | 2-Cyano-N-(4-cyanophenyl)-3-cyclopropyl-3-hydroxyprop-2-enamide | HCID 67659636 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70185499 | HCID 70185499 | — |
Reaction Steps
15 g (0.054 mol) of 2-cyano-3-cyclopropyl-3-hydroxyacrylic acid (4-cyanophenyl)amide are dissolved in 900 ml of water and 10 ml of ethanol together with 9.6 g (0.054 mol) of L-lysine hydrate, filtered and lyophilized. Adhering residual amounts of ethanol are removed by drying under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06020372 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-18708390ef644009b0355454abf396ae |
| Source note | uspto-grants-2000_02 |