Benzyl Bromide → HCID 19361963, compound

HRID 376446Notes

Reaction equation

BrBr.[F:3][C:4]1[CH:5]=[C:6]([CH3:11])[C:7](=[CH:9][CH:10]=1)[NH2:8].C([Br:19])C1C=CC=CC=1>>[F:3][C:4]1[CH:5]=[C:6]([CH3:11])[C:7](=[CH:9][CH:10]=1)[NH:8][Br:19]

Participants

Reactant 3

HCID 7498Benzyl Bromide

HCID 24408Bromine

HCID 679824-Fluoro-2-methylaniline

Product 1

HCID 19361963HCID 19361963, compound

Procedure

Bromine (0.5 mole) is added over 1 hour to stirred 4-fluoro-2-toluidine (0.5 mole) at 100° C. illuminated with a high wattage lamp. The crude benzyl bromide is used as prepared.

Workup

customilluminated with a high wattage lamp
customas prepared

Sources & evidence

ORD record: ord-79074d005420467787c7297c294513da
Source dataset: uspto-grants-2000_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06020379

Reaction notes

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