HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 19361955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Pentyl nitrite | HCID 10026 | — |
| Reactant | 5-Fluoro-o-toluidine | HCID 67774 | — |
| Product | HCID 19361955 | HCID 19361955 | — |
Reaction Steps
5-Fluorotoluidine (Example1,B), pyridine and pentyl nitrite are warmed until a vigorous reaction with evolution of gas sets in. This is allowed to proceed without heating until it has subsided (20 minutes) and the mixture is boiled under reflux for another 100 minutes. The excess pyridine is removed under reduced pressure to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06020379 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-41e13e5998024234b116bfe9284b909b |
| Source note | uspto-grants-2000_02 |