Diethylamine → HCID 5258522, compound

HRID 376643Notes

Reaction equation

HRID 376643 reaction equation
[F:1][C:2]([F:13])([F:12])[C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5](Cl)=[O:6].[CH2:14]([NH:16][CH2:17][CH3:18])[CH3:15]>>[CH2:14]([N:16]([CH2:17][CH3:18])[C:5](=[O:6])[C:4]1[CH:8]=[CH:9][CH:10]=[CH:11][C:3]=1[C:2]([F:13])([F:12])[F:1])[CH3:15]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 675612-(Trifluoromethyl)benzoyl chloride

Product 1

HCID 5258522HCID 5258522, compoundYield 97%

Procedure

N,N-Diethyl-2-(trifluoromethyl)benzamide was prepared from 2-trifluoromethylbenzoyl chloride and diethylamine according to General Method E1. No purification was needed to obtain 17.2 g of this compound, a 97% yield.

Workup

  1. customNo purification

Sources & evidence

ORD record
ord-2f02e427a0674d6ab44eb9ffcc622f16
Source dataset
uspto-grants-2000_02
Patent number
USRE036562

Reaction notes

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