HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 17683089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 3-(Trifluoromethyl)benzoic acid | HCID 9963 | — |
| Product | HCID 17683089 | HCID 17683089 | 19% |
Reaction Steps
3-Trifluoromethylbenzoic acid was converted to the acid chloride by the procedure of example b. The acid chloride was reacted with 70% aq ethylamine using General Method E1 to afford the title compound Purification by recrystallization from hexanes gave 2.24 g of N-ethyl-3-(trifluoromethyl)benzamide as a white needles in 19% yield. m.p. 98°-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE036562 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-6de2b85fd29e48d6aca82a77c675336a |
| Source note | uspto-grants-2000_02 |