HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 18630190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 17683089 | HCID 17683089 | — |
| Product | HCID 18630190 | HCID 18630190 | — |
Reaction Steps
This amide was reacted with TMSCl (1.3 eq) as in Example 221 to afford the title compound. The crude product was purified by RC (ethyl acetate/hexanes) and recrystallization from pentane (-78° C.) to afford 0.14 g (5%) of the title compound as a white solid. m.p. 101°-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE036562 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-4f4f05b5bb5244e79cb1ecf1862f228d |
| Source note | uspto-grants-2000_02 |