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HRID37675

反应详情

EQUATION

反应方程式

HRID 37675 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CCCN(C(CC)CC)[C@H]1COc2c(F)ccc(OS(=O)(=O)C(F)(F)F)c2C1
HCID54407297

未命名化合物

PRODUCTS

生成物

1
结构：CCCN(C(CC)CC)[C@H]1COc2c(F)ccc(OS(=O)(=O)C(F)(F)F)c2C1.Cl
HCID88370683

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

2 次

PROCEDURE

实验过程

(R)-8-Fluoro-3-(N-3-pentyl-N-n-propylamino)-5-trifluoromethanesulfonyloxychroman (100 mg, 0.23 mmol) was dissolved in ether. HCl in ether was added to precipitate the HCl-salt, and gave after drying 110 mg of (R)-8-fluoro-3-(N-3-pentyl-N-n-propylamino)-5-trifluoromethanesulfonyloxychroman hydrochloride as a white powder. Mp. 45°-60° C. (sinters).

WORKUP

后处理

  1. customto precipitate the HCl-salt
  2. customgave
  3. dry with materialafter drying 110 mg of (R)-8-fluoro-3-(N-3-pentyl-N-n-propylamino)-5-trifluoromethanesulfonyloxychroman hydrochloride as a white powder