HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17869403, compound → HCID 19359092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17869403 | HCID 17869403 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19359092 | HCID 19359092 | 60% |
Reaction Steps
The hydrogenation of 2.5 mmol of 5-(4-benzyloxy-2,3-difluorophenyl)-2-(6-dodecyloxypyridin-3-yl)pyrimidine in 50 ml of THF is carried out analogously to the procedure indicated for precursor 14, giving 0.7 g (60%) of a colorless solid, m.p. 111-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06022492 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-e3dc538d8da345a7bcf87edad2e7ac79 |
| Source note | uspto-grants-2000_02 |