Isopropanol → HCID 19359693, compound

Participants

Reaction Conditions

Reaction Steps

0.57 g of sodium (0.025 mol) was treated with 80 ml of isopropylalcohol in a 200 ml eggplant type flask and the mixture was heated at 60° C. until sodium was completely dissolved. To this solution 50 ml of an isopropylalcohol solution containing the 3-(trichlorostannyl)propylamine (4.9 mmol), prepared in the aforementioned example (4), was added dropwise at a room temperature. Subsequently, the mixture was stirred while heating for 6 hours at 70° C. The resultant supernatant was separated and concentrated under reduced pressure to yield 2.4 g of the final product of 3-aminopropyltin tris(methylethoxide) (yield=59%).

Provenance & Evidence