p-Anisoyl chloride → HCID 86749787, compound

HRID 377236Notes

Reaction equation

HRID 377236 reaction equation
C1(N[C:8]2[CH:13]=CC=CC=2N)C=CC=CC=1.[C:15]([Cl:25])(=[O:24])[C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1>C(OCC)C>[C:15]([Cl:25])(=[O:24])[C:16]1[CH:17]=[CH:18][C:19]([O:22][CH3:23])=[CH:20][CH:21]=1.[CH2:19]([O:22][CH2:13][CH3:8])[CH3:18]

Participants

4

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 68297N-Phenyl-o-phenylenediamine

Product 1

HCID 86749787HCID 86749787, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of N-phenyl-o-phenylenediamine (10 mmol, 1.84 g) in 100 ml diethyl ether was stirred at room temperature as p-anisoyl chloride (1 mmol, 1.71 g) was added dropwise. The resulting mixture was stirred at room temperature for about 96 hours. A precipitate formed before half of the anisoyl chloride/diethyl ether was added.

Workup

  1. additionwas added dropwise

Sources & evidence

ORD record
ord-ec7139594cde4ab4b11d89cb9d2c7a26
Source dataset
uspto-grants-2000_02
Patent number
US06025379

Reaction notes

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