HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 86749787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | N-Phenyl-o-phenylenediamine | HCID 68297 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86749787 | HCID 86749787 | — |
Reaction Steps
A solution of N-phenyl-o-phenylenediamine (10 mmol, 1.84 g) in 100 ml diethyl ether was stirred at room temperature as p-anisoyl chloride (1 mmol, 1.71 g) was added dropwise. The resulting mixture was stirred at room temperature for about 96 hours. A precipitate formed before half of the anisoyl chloride/diethyl ether was added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025379 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-ec7139594cde4ab4b11d89cb9d2c7a26 |
| Source note | uspto-grants-2000_02 |