HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 2-(2-(Allyloxy)ethoxy)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Diethylene Glycol | HCID 8117 | — |
| Solvent | NaH THF | HCID 23694757 | — |
| Product | 2-(2-(Allyloxy)ethoxy)ethanol | HCID 84777 | 82% |
Reaction Steps
Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524104B1 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-4e69885985a74b1ca4a5f8fc798f2882 |
| Source note | uspto-grants-2013_09 |