HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-1-cyclopenten-1-yl]phenoxy]acetate → Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]cyclopentyl]phenoxy]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-1-cyclopenten-1-yl]phenoxy]acetate | HCID 54404203 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]cyclopentyl]phenoxy]acetate | HCID 53672804 | 79.7% |
Reaction Steps
To a solution of ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-1-cyclopenten-1-yl]phenoxy]acetate (0.5 g) in ethanol (20 ml) was added 10% palladium on carbon (100 mg). After being stirred for 6 hours under hydrogen atmosphere, the reaction mixture was filtered. The solvent was evaporated in vacuo to give ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]cyclopentyl]phenoxy]acetate (400 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025375 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-3293a34090c84f3ba6e0a643fba58491 |
| Source note | uspto-grants-2000_02 |