HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86755140, compound → Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-2-hydroxycyclopentyl]phenoxy]-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86755140 | HCID 86755140 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-2-hydroxycyclopentyl]phenoxy]-acetate | HCID 86755141 | 51.8% |
Reaction Steps
To a solution of ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-1,2-epoxycyclopentyl]phenoxy]acetate (500 mg) in ethanol (20 ml) was added palladium on carbon (0.5 g). After being stirred for 24 hours under hydrogen atmosphere, the reaction mixture was filtered. The solvent was evaporated in vacuo to give ethyl [3-[2-[(4,5-diphenyloxazol-2-yl)methyl]-2-hydroxycyclopentyl]phenoxy]-acetate (260 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025375 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-a338e07cd94d4b6bb4538b8ecd013b19 |
| Source note | uspto-grants-2000_02 |