HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 44399137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86755139 | HCID 86755139 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44399137 | HCID 44399137 | — |
Reaction Steps
To a solution of (+)-methyl [3-[[(1S)-2-(4,5-diphenyloxazol-2-yl)-2-cyclopenten-1-yl]methyl]phenoxy]acetate (1.92 g) in ethanol (30 ml) was added 1N-aqueous sodium hydroxide (4.1 ml). The reaction mixture was stirred for 1 hour at room temperature. Ether (50 ml) was added to the solution. The precipitated solid was collected by filtration to afford (+)-sodium [3-[[(1S)-2-(4,5-diphenyloxazol-2-yl)-2-cyclopenten-1-yl]methyl]phenoxy]acetate (0.83 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025375 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-0a54bc4df4c44326a141ff2a89b8950a |
| Source note | uspto-grants-2000_02 |