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HRID37743

反应详情

EQUATION

反应方程式

HRID 37743 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccc(Oc2ccc(I)cc2)cc1
HCID21705773

未命名化合物

结构：CC(C)(C)OC(=O)CN(CC(=O)OC(C)(C)C)S(=O)(=O)c1ccc(Oc2ccccc2)cc1
HCID66916713

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CN(CC(=O)OC(C)(C)C)S(=O)(=O)c1ccc(Oc2ccc(I)cc2)cc1
HCID66916719

未命名化合物

PROCEDURE

实验过程

Compound 4e was prepared following the procedure described for 4a with reagent quantities adapted to the amount of starting material 3e (0.71 g, 1.81 mmol). Yield: 1.04 g, 1.64 mmol, 99% (white solid). 1H-NMR (DMSO-d6): δ 7.96 (d, 3J=8.5 Hz, 2H, ArH), 7.59 (d, 3J=8.5 Hz, 2H, ArH), 4.07 (s, 4H, 2×CH2CO2H), 1.40 (s, 18H, 2×CO2tBu).