Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 19358835 | HCID 19358835 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19358829 | HCID 19358829 | — |
Reaction Steps
4,9-Diethyl-2-(2-ethyl-1H-imidazol-1-yl)imidazo[5,1-h]pteridin-6(5H)-one (5.0 g, 15 mmol) is heated with 50 g of imidazole at 200° C. under N2 for 16 hours. The reaction mixture is cooled to -100° C. and 150 mL of methanol is added. The solids are filtered and washed with methanol to provide 4,9-diethyl-2-(1H-imidazol-1-yl)imidazo[5,1-h]pteridin-6(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06025489 |
|---|
| Source dataset | uspto-grants-2000_02 |
|---|
| ORD ID | ord-288afe3da129412392be65d4d62b7cc0 |
|---|
| Source note | uspto-grants-2000_02 |
|---|
