HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19358868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19358862 | HCID 19358862 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 19358868 | HCID 19358868 | — |
Reaction Steps
Prepared by hydrogenation of the product of Example 19 with palladium on carbon in ethanol containing 2 eq. NaOH, at 50 psi and 50° C. for 24 hours. The catalyst was removed and the product was precipitated by addition of a saturated solution of ammonium chloride. The solids were filtered and washed with water and ethanol to provide 9-ethyl-4-(methylamino)imidazo[5,1-h]pteridin-6(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025489 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-72de3ea056b249ccb286e2b325c6def6 |
| Source note | uspto-grants-2000_02 |