HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1,2-propanediol → HCID 19358861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1,2-propanediol | HCID 73561 | — |
| Reactant | HCID 19358842 | HCID 19358842 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 19358861 | HCID 19358861 | — |
Reaction Steps
Prepared by the treatment of the product of Example 41b with 10 eq. of 3-amino-1,2-propanediol in N-methylpyrrolidinone at 100° C. for 18 hours. The mixture was poured on water to precipitate the product. The solids were filtered, washed with water, and then acetonitrile, to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025489 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-af2717f248bd4f7691b2140540cd3697 |
| Source note | uspto-grants-2000_02 |