反应详情

A mixture of 8-bromo-9-benzyladenine (910 mg, 3.0 mmol), sodium hydrosulfide (1.08 g), and ethanol (50 ml) was refluxed for 12 h. After removal of solvent, the residue was dissolved into water and neutralized by 1 N HCl to obtain the desired compound as crystals (770 mg, Yield: 99%).

1. temperaturewas refluxed for 12 h
2. customAfter removal of solvent
3. dissolutionthe residue was dissolved into water