HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydrosulfide → HCID 178508658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydrosulfide | HCID 28015 | — |
| Reactant | 9-Benzyl-8-bromoadenine | HCID 9904551 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178508658 | HCID 178508658 | 99.7% |
Reaction Steps
A mixture of 8-bromo-9-benzyladenine (910 mg, 3.0 mmol), sodium hydrosulfide (1.08 g), and ethanol (50 ml) was refluxed for 12 h. After removal of solvent, the residue was dissolved into water and neutralized by 1 N HCl to obtain the desired compound as crystals (770 mg, Yield: 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028076 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-e5c58f9a80d74a1c9b82a77493f265a4 |
| Source note | uspto-grants-2000_02 |