HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86755157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 70289119 | HCID 70289119 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86755157 | HCID 86755157 | — |
Reaction Steps
(Z)-1-(p-methylthiobenzylidene)-5-dimethylamino-2-methyl-3-indenylacetic acid (70 mmol) in THF (500 ml) is allowed to react with oxalylchloride (2 M in CH2Cl2 ; 70 mmol) under reflux conditions (24 hours). The solvent is evaporated to yield the title compound, which is used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028116 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-8ddbd1becdaa4d3e954d8d4dfd4e0a54 |
| Source note | uspto-grants-2000_02 |