HRID37823

反应详情

EQUATION

反应方程式

HRID 37823 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 1-(2-cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.65 g, 12.9 mmol) in methanol (25 mL) was hydrogenated over 10% Pd/C (180 mg). After completion of the reaction the catalyst was removed by filtration, washing with methanol, and concentration of the filtrate gave 1-(2-cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.4 g, 93%).

WORKUP

后处理

  1. customAfter completion of the reaction the catalyst
  2. customwas removed by filtration
  3. washwashing with methanol, and concentration of the filtrate