HRID37823
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 1-(2-cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.65 g, 12.9 mmol) in methanol (25 mL) was hydrogenated over 10% Pd/C (180 mg). After completion of the reaction the catalyst was removed by filtration, washing with methanol, and concentration of the filtrate gave 1-(2-cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.4 g, 93%).
WORKUP
后处理
- customAfter completion of the reaction the catalyst
- customwas removed by filtration
- washwashing with methanol, and concentration of the filtrate