HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt → 1-(2-Cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt | HCID 86639594 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(2-Cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt | HCID 86639592 | 93% |
Reaction Steps
A solution of 1-(2-cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.65 g, 12.9 mmol) in methanol (25 mL) was hydrogenated over 10% Pd/C (180 mg). After completion of the reaction the catalyst was removed by filtration, washing with methanol, and concentration of the filtrate gave 1-(2-cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.4 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524705B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-98f63a28bdf942adaa9d24aceda54a07 |
| Source note | uspto-grants-2013_09 |