HCID 19353305, compound → HCID 19353328, compound

Participants

Reaction Steps

To an ethyl acetate (2 ml) solution of Benzyl 3-[10-(1,3-benzodioxol-5-yl)-8,9-dihydro-7H-1,3-benzodioxolo[4,5-f]isoindol-7-one-8-yl]carbonyl-propionate (50 mg) was added 10% palladium carbon (10 mg) and stirred overnight under hydrogen atmosphere. The catalysts were filtered off and the filtrate was concentrated under reduced pressure, then recrystallized from ethyl acetate-hexane to give the entitled compound (28 mg) as colorless crystals.

Provenance & Evidence