HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19353280, compound → HCID 19353399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19353280 | HCID 19353280 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19353399 | HCID 19353399 | — |
Reaction Steps
To a methanol (20 ml) solution of 8,9-dihydro-10-(4-pyridyl)-7H-1,3-benzodioxolo[4,5-f]isoindol-7-one (120 mg) was added 4N hydrogen chloride-ethyl acetate solution (4 ml) and stirred for 30 minutes. The resultant precipitates were collected by suction and washed with ethyl acetate to give the entitled compound (126 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030967 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-b16246ab7c524a94b702483f4d2672b6 |
| Source note | uspto-grants-2000_02 |