HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19353310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19353280 | HCID 19353280 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19353310 | HCID 19353310 | — |
Reaction Steps
To a methanol (10 ml) solution of 8,9-dihydro-10-(4-pyridyl)-7H-1,3-benzodioxolo[4,5-f]isoindol-7-one (63 mg) was added methyl iodide (3 ml) and heated under reflux for 3 hours. The resultant precipitates were collected by suction and recrystallized from methanol-THF to give the entitled compound (51 mg) as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030967 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-05cf7c17698f4b678ff2764540412f62 |
| Source note | uspto-grants-2000_02 |