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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 378257Generated: October 30, 2026

Methyl iodide → HCID 19353310, compound

https://huagongshe.com/reaction/378257

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 19353280HCID 19353280—
SolventMethanolHCID 887—
ProductHCID 19353310HCID 19353310—

Reaction Steps

To a methanol (10 ml) solution of 8,9-dihydro-10-(4-pyridyl)-7H-1,3-benzodioxolo[4,5-f]isoindol-7-one (63 mg) was added methyl iodide (3 ml) and heated under reflux for 3 hours. The resultant precipitates were collected by suction and recrystallized from methanol-THF to give the entitled compound (51 mg) as yellow crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06030967
Source datasetuspto-grants-2000_02
ORD IDord-05cf7c17698f4b678ff2764540412f62
Source noteuspto-grants-2000_02