HRID37827

反应详情

EQUATION

反应方程式

HRID 37827 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2-Cyclopentyl-indolizine (0.25 g, 1.35 mmol) was dissolved in methanol (5 mL) and hydrogenated over Raney nickel (50 mg) under balloon pressure at room temperature for 1 h. The reaction mixture was filtered through celite, washing with methanol. Concentration of the filtrate afforded 2-cyclopentyl-5,6,7,8-tetrahydro-indolizine (0.24 g, 94%) as a solid.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through celite
  2. washwashing with methanol