HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 5-(Aminomethyl)picolinonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 5-(Azidomethyl)pyridine-2-carbonitrile | HCID 21904627 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-(Aminomethyl)picolinonitrile | HCID 11355715 | — |
Reaction Steps
The compound obtained in (a) was dissolved in 45 ml of THF and 1.2 ml of water and, while stirring, 11.2 g of triphenylphosphine were added in portions. The reaction mixture was left to stand at RT overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030972 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-fb628f809a2147b79c012191bce5f78c |
| Source note | uspto-grants-2000_02 |