HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 15388686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 19353966 | HCID 19353966 | — |
| Reactant | HCID 50937077 | HCID 50937077 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15388686 | HCID 15388686 | — |
Reaction Steps
The title compound was prepared by first adding morpholine (1.02 g, 11.77 mmol) and the compound of Example 97, supra, (0.39 g, 1.00 mmol) to 125 ml of acetonitrile while stirring under nitrogen purge. To this mixture is then added diisopropylethyl aniline (1.51 ml, 8.67 mmol) dropwise. This reaction mixture is then allowed to stir overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030992 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-520e454afca0463e89bedb29367d56ea |
| Source note | uspto-grants-2000_02 |