HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18349749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | HCID 18349573 | HCID 18349573 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18349749 | HCID 18349749 | — |
Reaction Steps
In a similar manner to Example 71, a solution of butanesulphonyl chloride (0.45 g) in dichloromethane (5 ml) was added in portions over 5 minutes to a solution of 4-{1-[3-(imidazol-1-yl)propylamino]-1-methylethyl}phenol (0.75 g) and triethylamine (0.29 g) in dicloloromethane (5 ml) at 0° C. with stirring, to give 4-{1-[3-(imidazol-1-yl)propylamino]-1-methylethyl}phenyl 1-butanesulphonate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06031109 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-81d106117fc64d1a85570652902686ec |
| Source note | uspto-grants-2000_02 |