1-Phenylpiperazine → HCID 21697170, compound

HRID 378929Notes

Reaction equation

HRID 378929 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][CH2:12][C:13]([OH:15])=[O:14])(=[O:10])=[O:9])=[CH:4][CH:3]=1.[C:16]1([N:22]2[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]2)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[C:16]1([N:22]2[CH2:27][CH2:26][N:25]([C:2]3[CH:7]=[CH:6][C:5]([S:8]([NH:11][CH2:12][C:13]([OH:15])=[O:14])(=[O:10])=[O:9])=[CH:4][CH:3]=3)[CH2:24][CH2:23]2)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 70961-PhenylpiperazineHCID 7302692-(4-fluorophenylsulfonamido)acetic acid

Product 1

HCID 21697170HCID 21697170, compound

Procedure

In a manner similar to Example 3(b), (4-fluoro-benzenesulfonylamino)-acetic acid was condensed with 4-phenyl-piperazine to give the title compound, mp=120-124° C.

Sources & evidence

ORD record
ord-fb20af8875284a639a922fd5d042e129
Source dataset
uspto-grants-2001_10
Patent number
US06297247B1

Reaction notes

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