HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178514071, compound → HCID 178514069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178514071 | HCID 178514071 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178514069 | HCID 178514069 | 103.2% |
Reaction Steps
A solution of 3-trifluoromethylphenyl-4-nitro-2-(5-tetrazolyl)phenyl urea (0.8 g, 2.0 mmol) in 96% ethanol was hydrogenated over 5% palladium on charcoal for 3 hours at room temperature. The reaction mixture was filtered through a pad of celite and the solvent evaporated off to give 0.75 g of the desired product. M.p. 175-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297261B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-2b40284544454a90bdd10c8cc3b141e6 |
| Source note | uspto-grants-2001_10 |