HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 54164352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | HCID 21697292 | HCID 21697292 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54164352 | HCID 54164352 | 49% |
Reaction Steps
Operating analogously to example 2 using 2-(5-phenylpentyloxy)-3-methoxy-benzaldehyde (1 g, 3.35 mmoles), obtained as described in example 12, 8.03M methylamine in ethanol (0.088 ml, 0.7035 mmoles), acetic acid (0.04 ml, 0.7035 mmoles) and nitromethane (0.198 ml, 3.685 mmoles) in methanol (5 ml), 0.56 g of the title product was obtained (yield: 49%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297257B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-cd5f292f5a484da6849c6c6c5462afba |
| Source note | uspto-grants-2001_10 |