HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21697270, compound → HCID 21697269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21697270 | HCID 21697270 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21697269 | HCID 21697269 | 75% |
Reaction Steps
Operating analogously to example 31 using 1-(3-cyclopentyloxy-4-methoxy-6-nitro-phenyl)-2-(3,5-dichloro-pyridin-4-yl-methyl)-ethanone (26.75 g, 63 moles), obtained as described in example 38, and iron dust (21.1 g, 378 moles) in acetic acid (120 ml) 18.7 g of the title product were obtained (yield: 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297257B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-2dbcbb56a27648859a8a4e269a9150db |
| Source note | uspto-grants-2001_10 |